A 3.650-g sample containing bromate and bromide was dissolved in sufficient water to give
290.0 mL. After acidification, silver nitrate was introduced to a 25.00-mL aliquot to precipitate
AgBr, which was fil- tered, washed, and then redissolved in an ammoniacal solution of potassium
tetracyanonickelate(II)
Ni(CN)42- + 2 AgBr(s) → 2Ag(CN)2- + Ni2+ + 12Br-
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