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Answer to Question #76566 in Organic Chemistry for george
Question #76566
SINCE Phenylalanine is reduced to Phenylalaninol in 16-18 hours under reflux with Sodium Borohydride and Sulfuric Acid in Dry Tetrahydrofuran.My question is to reduce 100gr of phenylalanine how much sodium borohydride and sulfuric acid is need?and in how many ml of dry thf must refluxed ? And after reflux i can remove the sodium borohydride with a filtration and and the thf/sulfuric acid/phenylalanine batch neutralised with NAOH and Phenylalaninol extracted with Toluen?
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