Volhard method In an experiment of determination of KBr (g%) by volhard method In a flask; - 15ml KBr was taken - 25 ml 0.05M AgNO3 - 1 ml nitric acid - 1 ml ferric alum indicator Then titration with 0.05M KSCN was done - The end point was =15 ml • Calculate the mass of KBr in g%
Ag+ + Cl– ⇾ AgCl
Ag+ + SCN– ⇾ AgSCN
SCN– + Fe3+ ⇾ FeSCN
15×100=15%
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